Validation method of cis and trans fatty acids determination in vegetable oils using gas chromatography for food products

Yus Maria Novelina; Sumi Hudiyono

doi:10.1063/1.5065057

Validation method of cis and trans fatty acids determination in vegetable oils using gas chromatography for food products

Yus Maria Novelina, Sumi Hudiyono

Department of Chemistry

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

Abstract

Trans fatty acid content in food products might have impacts to human health. The labelling policy particularly on trans fatty acid (TFA) on food products has created a demand on a quick method that can be used to determine trans fatty acid low content in food products. The testing method used in this research is from International Olive Oil Council (IOOC) to determine TFA<1% in vegetable oil. In order to see the performance of the method used in the testing, a validation of the method is conducted. The result from method validation showed that detection limit values was 0.05% and % recovery of the certified reference material BCR 162 used as matrixes was within the range of 68-106%, meanwhile % precision was within the range of 0.1%-13.7%. Hence, the validation of IOOC method on cis and trans fatty acids of vegetable oil determination using chromatography gas (TCR-CN100 60 m x 0.25 mm x 0.2 μm) with FID detector showed that the testing method can be used to determine cis and fatty acids<1% in oils/fats. This method has been applied in the testing some commercial vegetable oils available in the market (palm, sunflower, soybean, coconut, and corn oils). The results were not significantly different from the reference standard.

Original language	English
Title of host publication	2nd International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2018
Editors	Is Fatimah, M. Arsyik Kurniawan S., Imam Sahroni, Laemthong Chuenchom, Miqdam Musawwa, Hideya Kawasaki, Azlan Kamari
Publisher	American Institute of Physics Inc.
ISBN (Electronic)	9780735417465
DOIs	https://doi.org/10.1063/1.5065057
Publication status	Published - 29 Oct 2018
Event	2nd International Conference on Chemistry, Chemical Process and Engineering 2018, IC3PE 2018 - Yogyakarta, Indonesia Duration: 14 Aug 2018 → …

Publication series

Name	AIP Conference Proceedings
Volume	2026
ISSN (Print)	0094-243X
ISSN (Electronic)	1551-7616

Conference

Conference	2nd International Conference on Chemistry, Chemical Process and Engineering 2018, IC3PE 2018
Country/Territory	Indonesia
City	Yogyakarta
Period	14/08/18 → …

UN SDGs

This output contributes to the following UN Sustainable Development Goals (SDGs)

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10.1063/1.5065057

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Novelina, Y. M., & Hudiyono, S. (2018). Validation method of cis and trans fatty acids determination in vegetable oils using gas chromatography for food products. In I. Fatimah, M. A. Kurniawan S., I. Sahroni, L. Chuenchom, M. Musawwa, H. Kawasaki, & A. Kamari (Eds.), 2nd International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2018 Article 020097 (AIP Conference Proceedings; Vol. 2026). American Institute of Physics Inc.. https://doi.org/10.1063/1.5065057

Novelina, Yus Maria ; Hudiyono, Sumi. / Validation method of cis and trans fatty acids determination in vegetable oils using gas chromatography for food products. 2nd International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2018. editor / Is Fatimah ; M. Arsyik Kurniawan S. ; Imam Sahroni ; Laemthong Chuenchom ; Miqdam Musawwa ; Hideya Kawasaki ; Azlan Kamari. American Institute of Physics Inc., 2018. (AIP Conference Proceedings).

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abstract = "Trans fatty acid content in food products might have impacts to human health. The labelling policy particularly on trans fatty acid (TFA) on food products has created a demand on a quick method that can be used to determine trans fatty acid low content in food products. The testing method used in this research is from International Olive Oil Council (IOOC) to determine TFA<1% in vegetable oil. In order to see the performance of the method used in the testing, a validation of the method is conducted. The result from method validation showed that detection limit values was 0.05% and % recovery of the certified reference material BCR 162 used as matrixes was within the range of 68-106%, meanwhile % precision was within the range of 0.1%-13.7%. Hence, the validation of IOOC method on cis and trans fatty acids of vegetable oil determination using chromatography gas (TCR-CN100 60 m x 0.25 mm x 0.2 μm) with FID detector showed that the testing method can be used to determine cis and fatty acids<1% in oils/fats. This method has been applied in the testing some commercial vegetable oils available in the market (palm, sunflower, soybean, coconut, and corn oils). The results were not significantly different from the reference standard.",

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Novelina, YM & Hudiyono, S 2018, Validation method of cis and trans fatty acids determination in vegetable oils using gas chromatography for food products. in I Fatimah, MA Kurniawan S., I Sahroni, L Chuenchom, M Musawwa, H Kawasaki & A Kamari (eds), 2nd International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2018., 020097, AIP Conference Proceedings, vol. 2026, American Institute of Physics Inc., 2nd International Conference on Chemistry, Chemical Process and Engineering 2018, IC3PE 2018, Yogyakarta, Indonesia, 14/08/18. https://doi.org/10.1063/1.5065057

Validation method of cis and trans fatty acids determination in vegetable oils using gas chromatography for food products. / Novelina, Yus Maria; Hudiyono, Sumi.
2nd International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2018. ed. / Is Fatimah; M. Arsyik Kurniawan S.; Imam Sahroni; Laemthong Chuenchom; Miqdam Musawwa; Hideya Kawasaki; Azlan Kamari. American Institute of Physics Inc., 2018. 020097 (AIP Conference Proceedings; Vol. 2026).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

TY - GEN

T1 - Validation method of cis and trans fatty acids determination in vegetable oils using gas chromatography for food products

AU - Novelina, Yus Maria

AU - Hudiyono, Sumi

PY - 2018/10/29

Y1 - 2018/10/29

N2 - Trans fatty acid content in food products might have impacts to human health. The labelling policy particularly on trans fatty acid (TFA) on food products has created a demand on a quick method that can be used to determine trans fatty acid low content in food products. The testing method used in this research is from International Olive Oil Council (IOOC) to determine TFA<1% in vegetable oil. In order to see the performance of the method used in the testing, a validation of the method is conducted. The result from method validation showed that detection limit values was 0.05% and % recovery of the certified reference material BCR 162 used as matrixes was within the range of 68-106%, meanwhile % precision was within the range of 0.1%-13.7%. Hence, the validation of IOOC method on cis and trans fatty acids of vegetable oil determination using chromatography gas (TCR-CN100 60 m x 0.25 mm x 0.2 μm) with FID detector showed that the testing method can be used to determine cis and fatty acids<1% in oils/fats. This method has been applied in the testing some commercial vegetable oils available in the market (palm, sunflower, soybean, coconut, and corn oils). The results were not significantly different from the reference standard.

AB - Trans fatty acid content in food products might have impacts to human health. The labelling policy particularly on trans fatty acid (TFA) on food products has created a demand on a quick method that can be used to determine trans fatty acid low content in food products. The testing method used in this research is from International Olive Oil Council (IOOC) to determine TFA<1% in vegetable oil. In order to see the performance of the method used in the testing, a validation of the method is conducted. The result from method validation showed that detection limit values was 0.05% and % recovery of the certified reference material BCR 162 used as matrixes was within the range of 68-106%, meanwhile % precision was within the range of 0.1%-13.7%. Hence, the validation of IOOC method on cis and trans fatty acids of vegetable oil determination using chromatography gas (TCR-CN100 60 m x 0.25 mm x 0.2 μm) with FID detector showed that the testing method can be used to determine cis and fatty acids<1% in oils/fats. This method has been applied in the testing some commercial vegetable oils available in the market (palm, sunflower, soybean, coconut, and corn oils). The results were not significantly different from the reference standard.

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BT - 2nd International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2018

A2 - Fatimah, Is

A2 - Kurniawan S., M. Arsyik

A2 - Sahroni, Imam

A2 - Chuenchom, Laemthong

A2 - Musawwa, Miqdam

A2 - Kawasaki, Hideya

A2 - Kamari, Azlan

PB - American Institute of Physics Inc.

T2 - 2nd International Conference on Chemistry, Chemical Process and Engineering 2018, IC3PE 2018

Y2 - 14 August 2018

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Novelina YM, Hudiyono S. Validation method of cis and trans fatty acids determination in vegetable oils using gas chromatography for food products. In Fatimah I, Kurniawan S. MA, Sahroni I, Chuenchom L, Musawwa M, Kawasaki H, Kamari A, editors, 2nd International Conference on Chemistry, Chemical Process and Engineering, IC3PE 2018. American Institute of Physics Inc. 2018. 020097. (AIP Conference Proceedings). doi: 10.1063/1.5065057

Validation method of cis and trans fatty acids determination in vegetable oils using gas chromatography for food products

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