Utilization of eggshell-derived material as a solid base catalyst for efficient synthesis of substituted chalcones

Lina Mardiana; Bayu Ardiansah; Ridla Bakri; Antonius Herry Cahyana; Yulia Anita; Nuraini Pahlawati Aziza

doi:10.11113/jt.v79.10220

Utilization of eggshell-derived material as a solid base catalyst for efficient synthesis of substituted chalcones

Lina Mardiana, Bayu Ardiansah, Ridla Bakri, Antonius Herry Cahyana, Yulia Anita, Nuraini Pahlawati Aziza

Department of Chemistry

Research output: Contribution to journal › Article › peer-review

9 Citations (Scopus)

Abstract

A simple preparation of sodium impregnated on activated chicken eggshells (Na-ACE) as a solid base material for substituted chalcones synthesis is presented. After characterization using FTIR, XRD, SEM, EDS and total basicity, the catalyst was applied in Aldol condensation to produce corresponding chalcones 3a-3j. Confirmation of products structure has been done by FTIR, UV-Vis and MS instruments. Reaction can be carried out in relative short time with ethanol as the best solvent and gave the highest yield of 95 %. This research presented a facile synthesis of chalcone derivatives, the prominent class of organic compounds with interesting biological activities.

Original language	English
Pages (from-to)	175-182
Number of pages	8
Journal	Jurnal Teknologi
Volume	79
Issue number	5
DOIs	https://doi.org/10.11113/jt.v79.10220
Publication status	Published - Jul 2017

Keywords

Activated chicken eggshells
Aldol condensation
Chalcones

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10.11113/jt.v79.10220

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abstract = "A simple preparation of sodium impregnated on activated chicken eggshells (Na-ACE) as a solid base material for substituted chalcones synthesis is presented. After characterization using FTIR, XRD, SEM, EDS and total basicity, the catalyst was applied in Aldol condensation to produce corresponding chalcones 3a-3j. Confirmation of products structure has been done by FTIR, UV-Vis and MS instruments. Reaction can be carried out in relative short time with ethanol as the best solvent and gave the highest yield of 95 %. This research presented a facile synthesis of chalcone derivatives, the prominent class of organic compounds with interesting biological activities.",

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AU - Mardiana, Lina

AU - Ardiansah, Bayu

AU - Bakri, Ridla

AU - Cahyana, Antonius Herry

AU - Anita, Yulia

AU - Aziza, Nuraini Pahlawati

PY - 2017/7

Y1 - 2017/7

N2 - A simple preparation of sodium impregnated on activated chicken eggshells (Na-ACE) as a solid base material for substituted chalcones synthesis is presented. After characterization using FTIR, XRD, SEM, EDS and total basicity, the catalyst was applied in Aldol condensation to produce corresponding chalcones 3a-3j. Confirmation of products structure has been done by FTIR, UV-Vis and MS instruments. Reaction can be carried out in relative short time with ethanol as the best solvent and gave the highest yield of 95 %. This research presented a facile synthesis of chalcone derivatives, the prominent class of organic compounds with interesting biological activities.

AB - A simple preparation of sodium impregnated on activated chicken eggshells (Na-ACE) as a solid base material for substituted chalcones synthesis is presented. After characterization using FTIR, XRD, SEM, EDS and total basicity, the catalyst was applied in Aldol condensation to produce corresponding chalcones 3a-3j. Confirmation of products structure has been done by FTIR, UV-Vis and MS instruments. Reaction can be carried out in relative short time with ethanol as the best solvent and gave the highest yield of 95 %. This research presented a facile synthesis of chalcone derivatives, the prominent class of organic compounds with interesting biological activities.

KW - Activated chicken eggshells

KW - Aldol condensation

KW - Chalcones

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ER -

Utilization of eggshell-derived material as a solid base catalyst for efficient synthesis of substituted chalcones

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Keywords

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