TY - JOUR
T1 - Utilization of eggshell-derived material as a solid base catalyst for efficient synthesis of substituted chalcones
AU - Mardiana, Lina
AU - Ardiansah, Bayu
AU - Bakri, Ridla
AU - Cahyana, Antonius Herry
AU - Anita, Yulia
AU - Aziza, Nuraini Pahlawati
PY - 2017/7/1
Y1 - 2017/7/1
N2 - A simple preparation of sodium impregnated on activated chicken eggshells (Na-ACE) as a solid base material for substituted chalcones synthesis is presented. After characterization using FTIR, XRD, SEM, EDS and total basicity, the catalyst was applied in Aldol condensation to produce corresponding chalcones 3a-3j. Confirmation of products structure has been done by FTIR, UV-Vis and MS instruments. Reaction can be carried out in relative short time with ethanol as the best solvent and gave the highest yield of 95 %. This research presented a facile synthesis of chalcone derivatives, the prominent class of organic compounds with interesting biological activities.
AB - A simple preparation of sodium impregnated on activated chicken eggshells (Na-ACE) as a solid base material for substituted chalcones synthesis is presented. After characterization using FTIR, XRD, SEM, EDS and total basicity, the catalyst was applied in Aldol condensation to produce corresponding chalcones 3a-3j. Confirmation of products structure has been done by FTIR, UV-Vis and MS instruments. Reaction can be carried out in relative short time with ethanol as the best solvent and gave the highest yield of 95 %. This research presented a facile synthesis of chalcone derivatives, the prominent class of organic compounds with interesting biological activities.
KW - Activated chicken eggshells
KW - Aldol condensation
KW - Chalcones
UR - http://www.scopus.com/inward/record.url?scp=85021157693&partnerID=8YFLogxK
U2 - 10.11113/jt.v79.10220
DO - 10.11113/jt.v79.10220
M3 - Article
AN - SCOPUS:85021157693
VL - 79
SP - 175
EP - 182
JO - Jurnal Teknologi (Sciences and Engineering)
JF - Jurnal Teknologi (Sciences and Engineering)
SN - 0127-9696
IS - 5
ER -