The Synthesis of Gold Nanoparticles with Allyl Mercaptan as the Capping Agent to Modify Boron-Doped Diamond Surface for An Application As Oxygen Sensors

Wellson A. Kurniawan; Aminah Umar; Tribidasari A. Ivandini

doi:10.1109/ISSIMM.2018.8727741

The Synthesis of Gold Nanoparticles with Allyl Mercaptan as the Capping Agent to Modify Boron-Doped Diamond Surface for An Application As Oxygen Sensors

Wellson A. Kurniawan, Aminah Umar, Tribidasari A. Ivandini

Department of Chemistry

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

2 Citations (Scopus)

Abstract

In order to increase the conductivity and sensitivity of boron-doped diamond (BDD) electrodes for oxygen sensors application, modification with gold nanoparticles (AuNPs) was performed. This study aims to synthesize AuNPs using allyl mercaptan as the capping agent and employ the AuNPs to modify BDD electrodes. Characterization of the synthesized AuNPs by using UV-Vis spectrophotometer showed the specific gold nanoparticles wavelength at about 510 to 580 nm, while the characterization by using Particle Size Analyzer and Transmission Electron Microscopy (TEM) showed that AuNP formed particles with an average size of 11 ± 4 nm. Modification of BDD surface with the synthesized AuNPs by using immersion technique under UV irradiation resulted in homogeneously distributed of AuNPs at the BDD surface with Au:C ratio around 2:98. Preliminary study of the AuNPs-modified BDD to determine dissolved oxygen solutions by using cyclic voltammetry technique suggested that the sensor has comparable capability to gold bulk electrode.

Original language	English
Title of host publication	ISSIMM 2018 - 3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, Proceeding
Publisher	Institute of Electrical and Electronics Engineers Inc.
Pages	97-100
Number of pages	4
ISBN (Electronic)	9781728113692
DOIs	https://doi.org/10.1109/ISSIMM.2018.8727741
Publication status	Published - 1 Dec 2018
Event	3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, ISSIMM 2018 - Depok, Indonesia Duration: 4 Dec 2018 → 5 Dec 2018

Publication series

Name	ISSIMM 2018 - 3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, Proceeding

Conference

Conference	3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, ISSIMM 2018
Country/Territory	Indonesia
City	Depok
Period	4/12/18 → 5/12/18

Keywords

allyl mercaptan
boron-doped diamond
gold nanoparticles
oxygen sensor
surface modification

Access to Document

10.1109/ISSIMM.2018.8727741

Cite this

Kurniawan, W. A., Umar, A., & Ivandini, T. A. (2018). The Synthesis of Gold Nanoparticles with Allyl Mercaptan as the Capping Agent to Modify Boron-Doped Diamond Surface for An Application As Oxygen Sensors. In ISSIMM 2018 - 3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, Proceeding (pp. 97-100). Article 8727741 (ISSIMM 2018 - 3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, Proceeding). Institute of Electrical and Electronics Engineers Inc.. https://doi.org/10.1109/ISSIMM.2018.8727741

Kurniawan, Wellson A. ; Umar, Aminah ; Ivandini, Tribidasari A. / The Synthesis of Gold Nanoparticles with Allyl Mercaptan as the Capping Agent to Modify Boron-Doped Diamond Surface for An Application As Oxygen Sensors. ISSIMM 2018 - 3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, Proceeding. Institute of Electrical and Electronics Engineers Inc., 2018. pp. 97-100 (ISSIMM 2018 - 3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, Proceeding).

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title = "The Synthesis of Gold Nanoparticles with Allyl Mercaptan as the Capping Agent to Modify Boron-Doped Diamond Surface for An Application As Oxygen Sensors",

abstract = "In order to increase the conductivity and sensitivity of boron-doped diamond (BDD) electrodes for oxygen sensors application, modification with gold nanoparticles (AuNPs) was performed. This study aims to synthesize AuNPs using allyl mercaptan as the capping agent and employ the AuNPs to modify BDD electrodes. Characterization of the synthesized AuNPs by using UV-Vis spectrophotometer showed the specific gold nanoparticles wavelength at about 510 to 580 nm, while the characterization by using Particle Size Analyzer and Transmission Electron Microscopy (TEM) showed that AuNP formed particles with an average size of 11 ± 4 nm. Modification of BDD surface with the synthesized AuNPs by using immersion technique under UV irradiation resulted in homogeneously distributed of AuNPs at the BDD surface with Au:C ratio around 2:98. Preliminary study of the AuNPs-modified BDD to determine dissolved oxygen solutions by using cyclic voltammetry technique suggested that the sensor has comparable capability to gold bulk electrode.",

keywords = "allyl mercaptan, boron-doped diamond, gold nanoparticles, oxygen sensor, surface modification",

author = "Kurniawan, {Wellson A.} and Aminah Umar and Ivandini, {Tribidasari A.}",

year = "2018",

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doi = "10.1109/ISSIMM.2018.8727741",

language = "English",

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booktitle = "ISSIMM 2018 - 3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, Proceeding",

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note = "3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, ISSIMM 2018 ; Conference date: 04-12-2018 Through 05-12-2018",

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Kurniawan, WA, Umar, A & Ivandini, TA 2018, The Synthesis of Gold Nanoparticles with Allyl Mercaptan as the Capping Agent to Modify Boron-Doped Diamond Surface for An Application As Oxygen Sensors. in ISSIMM 2018 - 3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, Proceeding., 8727741, ISSIMM 2018 - 3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, Proceeding, Institute of Electrical and Electronics Engineers Inc., pp. 97-100, 3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, ISSIMM 2018, Depok, Indonesia, 4/12/18. https://doi.org/10.1109/ISSIMM.2018.8727741

The Synthesis of Gold Nanoparticles with Allyl Mercaptan as the Capping Agent to Modify Boron-Doped Diamond Surface for An Application As Oxygen Sensors. / Kurniawan, Wellson A.; Umar, Aminah ; Ivandini, Tribidasari A.
ISSIMM 2018 - 3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, Proceeding. Institute of Electrical and Electronics Engineers Inc., 2018. p. 97-100 8727741 (ISSIMM 2018 - 3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, Proceeding).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

TY - GEN

T1 - The Synthesis of Gold Nanoparticles with Allyl Mercaptan as the Capping Agent to Modify Boron-Doped Diamond Surface for An Application As Oxygen Sensors

AU - Kurniawan, Wellson A.

AU - Umar, Aminah

AU - Ivandini, Tribidasari A.

PY - 2018/12/1

Y1 - 2018/12/1

N2 - In order to increase the conductivity and sensitivity of boron-doped diamond (BDD) electrodes for oxygen sensors application, modification with gold nanoparticles (AuNPs) was performed. This study aims to synthesize AuNPs using allyl mercaptan as the capping agent and employ the AuNPs to modify BDD electrodes. Characterization of the synthesized AuNPs by using UV-Vis spectrophotometer showed the specific gold nanoparticles wavelength at about 510 to 580 nm, while the characterization by using Particle Size Analyzer and Transmission Electron Microscopy (TEM) showed that AuNP formed particles with an average size of 11 ± 4 nm. Modification of BDD surface with the synthesized AuNPs by using immersion technique under UV irradiation resulted in homogeneously distributed of AuNPs at the BDD surface with Au:C ratio around 2:98. Preliminary study of the AuNPs-modified BDD to determine dissolved oxygen solutions by using cyclic voltammetry technique suggested that the sensor has comparable capability to gold bulk electrode.

AB - In order to increase the conductivity and sensitivity of boron-doped diamond (BDD) electrodes for oxygen sensors application, modification with gold nanoparticles (AuNPs) was performed. This study aims to synthesize AuNPs using allyl mercaptan as the capping agent and employ the AuNPs to modify BDD electrodes. Characterization of the synthesized AuNPs by using UV-Vis spectrophotometer showed the specific gold nanoparticles wavelength at about 510 to 580 nm, while the characterization by using Particle Size Analyzer and Transmission Electron Microscopy (TEM) showed that AuNP formed particles with an average size of 11 ± 4 nm. Modification of BDD surface with the synthesized AuNPs by using immersion technique under UV irradiation resulted in homogeneously distributed of AuNPs at the BDD surface with Au:C ratio around 2:98. Preliminary study of the AuNPs-modified BDD to determine dissolved oxygen solutions by using cyclic voltammetry technique suggested that the sensor has comparable capability to gold bulk electrode.

KW - allyl mercaptan

KW - boron-doped diamond

KW - gold nanoparticles

KW - oxygen sensor

KW - surface modification

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U2 - 10.1109/ISSIMM.2018.8727741

DO - 10.1109/ISSIMM.2018.8727741

M3 - Conference contribution

T3 - ISSIMM 2018 - 3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, Proceeding

SP - 97

EP - 100

BT - ISSIMM 2018 - 3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, Proceeding

PB - Institute of Electrical and Electronics Engineers Inc.

T2 - 3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, ISSIMM 2018

Y2 - 4 December 2018 through 5 December 2018

ER -

Kurniawan WA, Umar A , Ivandini TA. The Synthesis of Gold Nanoparticles with Allyl Mercaptan as the Capping Agent to Modify Boron-Doped Diamond Surface for An Application As Oxygen Sensors. In ISSIMM 2018 - 3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, Proceeding. Institute of Electrical and Electronics Engineers Inc. 2018. p. 97-100. 8727741. (ISSIMM 2018 - 3rd International Seminar on Sensors, Instrumentation, Measurement and Metrology, Proceeding). doi: 10.1109/ISSIMM.2018.8727741

The Synthesis of Gold Nanoparticles with Allyl Mercaptan as the Capping Agent to Modify Boron-Doped Diamond Surface for An Application As Oxygen Sensors

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