The Preparation of Porous TiO2 Nanostructure by Triblock Copolymers Co-Templating Method of TiOSO4 Solution Derived from Ilmenite Ore

Akhmad Herman Yuwono; Latifa Hanum Lalasari; Amalia Sholehah

doi:10.4028/www.scientific.net/AMR.887-888.132

The Preparation of Porous TiO₂ Nanostructure by Triblock Copolymers Co-Templating Method of TiOSO₄ Solution Derived from Ilmenite Ore

Akhmad Herman Yuwono, Latifa Hanum Lalasari, Amalia Sholehah

Department of Metallurgical and Material Engineering

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

1 Citation (Scopus)

Abstract

Porous titanium dioxide (TiO₂) nanostructure has been successfully synthesized by a modified sol-gel method using non-ionic triblock copolymer pluronic F-127 as surfactant template and titanylsulfate (TiOSO₄) solution as the inorganic precursor derived from the sulfuric process of Bangka-Indonesia ilmenite ore. The resulting nanostructure samples were characterized by XRD, SEM, TEM and UV-Vis spectroscopy. The results showed that porous titania particles have sphere-like shape and can be indexed as the anatase phase with average crystallite size of about 5-7 nm, narrow pore size distribution with an averange pore diameter of about 3-5 nm and band gap energy in the range of 3.10 - 3.16 eV.

Original language	English
Title of host publication	Advances in Materials and Materials Processing IV
Pages	132-138
Number of pages	7
DOIs	https://doi.org/10.4028/www.scientific.net/AMR.887-888.132
Publication status	Published - 2014
Event	2013 4th International Conference on Advances in Materials and Manufacturing, ICAMMP 2013 - Kunming, China Duration: 18 Dec 2013 → 19 Dec 2013

Publication series

Name	Advanced Materials Research
Volume	887-888
ISSN (Print)	1022-6680

Conference

Conference	2013 4th International Conference on Advances in Materials and Manufacturing, ICAMMP 2013
Country/Territory	China
City	Kunming
Period	18/12/13 → 19/12/13

Keywords

Ilmenite
Pluronic F-127 surfactant
Porous TiO
Titanylsulfate

Access to Document

10.4028/www.scientific.net/AMR.887-888.132

Cite this

@inproceedings{d7539c1cf9c04cf4bb5918121f6cfa71,

title = "The Preparation of Porous TiO2 Nanostructure by Triblock Copolymers Co-Templating Method of TiOSO4 Solution Derived from Ilmenite Ore",

abstract = "Porous titanium dioxide (TiO2) nanostructure has been successfully synthesized by a modified sol-gel method using non-ionic triblock copolymer pluronic F-127 as surfactant template and titanylsulfate (TiOSO4) solution as the inorganic precursor derived from the sulfuric process of Bangka-Indonesia ilmenite ore. The resulting nanostructure samples were characterized by XRD, SEM, TEM and UV-Vis spectroscopy. The results showed that porous titania particles have sphere-like shape and can be indexed as the anatase phase with average crystallite size of about 5-7 nm, narrow pore size distribution with an averange pore diameter of about 3-5 nm and band gap energy in the range of 3.10 - 3.16 eV.",

keywords = "Ilmenite, Pluronic F-127 surfactant, Porous TiO, Titanylsulfate",

author = "Yuwono, {Akhmad Herman} and Lalasari, {Latifa Hanum} and Amalia Sholehah",

year = "2014",

doi = "10.4028/www.scientific.net/AMR.887-888.132",

language = "English",

isbn = "9783038350149",

series = "Advanced Materials Research",

pages = "132--138",

booktitle = "Advances in Materials and Materials Processing IV",

note = "2013 4th International Conference on Advances in Materials and Manufacturing, ICAMMP 2013 ; Conference date: 18-12-2013 Through 19-12-2013",

}

Yuwono, AH, Lalasari, LH & Sholehah, A 2014, The Preparation of Porous TiO₂ Nanostructure by Triblock Copolymers Co-Templating Method of TiOSO₄ Solution Derived from Ilmenite Ore. in Advances in Materials and Materials Processing IV. Advanced Materials Research, vol. 887-888, pp. 132-138, 2013 4th International Conference on Advances in Materials and Manufacturing, ICAMMP 2013, Kunming, China, 18/12/13. https://doi.org/10.4028/www.scientific.net/AMR.887-888.132

The Preparation of Porous TiO₂ Nanostructure by Triblock Copolymers Co-Templating Method of TiOSO₄ Solution Derived from Ilmenite Ore. / Yuwono, Akhmad Herman; Lalasari, Latifa Hanum; Sholehah, Amalia.
Advances in Materials and Materials Processing IV. 2014. p. 132-138 (Advanced Materials Research; Vol. 887-888).

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › peer-review

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AU - Lalasari, Latifa Hanum

AU - Sholehah, Amalia

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N2 - Porous titanium dioxide (TiO2) nanostructure has been successfully synthesized by a modified sol-gel method using non-ionic triblock copolymer pluronic F-127 as surfactant template and titanylsulfate (TiOSO4) solution as the inorganic precursor derived from the sulfuric process of Bangka-Indonesia ilmenite ore. The resulting nanostructure samples were characterized by XRD, SEM, TEM and UV-Vis spectroscopy. The results showed that porous titania particles have sphere-like shape and can be indexed as the anatase phase with average crystallite size of about 5-7 nm, narrow pore size distribution with an averange pore diameter of about 3-5 nm and band gap energy in the range of 3.10 - 3.16 eV.

AB - Porous titanium dioxide (TiO2) nanostructure has been successfully synthesized by a modified sol-gel method using non-ionic triblock copolymer pluronic F-127 as surfactant template and titanylsulfate (TiOSO4) solution as the inorganic precursor derived from the sulfuric process of Bangka-Indonesia ilmenite ore. The resulting nanostructure samples were characterized by XRD, SEM, TEM and UV-Vis spectroscopy. The results showed that porous titania particles have sphere-like shape and can be indexed as the anatase phase with average crystallite size of about 5-7 nm, narrow pore size distribution with an averange pore diameter of about 3-5 nm and band gap energy in the range of 3.10 - 3.16 eV.

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