The influence of calcination temperature on optical properties of ZnO nanoparticles

Iwan Sugihartono, Atika Retnoningtyas, Cecep Rustana, Umiatin, Nurfina Yudasari, Isnaeni, Cuk Imawan, Fera Kurniadewi

Research output: Chapter in Book/Report/Conference proceedingConference contributionpeer-review

2 Citations (Scopus)

Abstract

ZnO nanoparticles (NPs) have synthesized by sol-gel with different calcination temperatures. Scanning electron microscopy (SEM) shows that the morphology of ZnO NPs has large aggregation. Then, X-ray diffraction (XRD) technique confirmed that the XRD pattern of ZnO NPs has polycrystalline wurtzite structure. The crystallite size in (002) plane at a calcination temperature of 200 °C, 400 °C, 600 °C are 9.28nm, 12.60nm, 20.11nm, respectively. The intensity of observed peaks increases when the calcination temperature is higher. The room temperature UV-Vis absorbance of ZnO NPs indicate that the higher calcination temperature cause absorption peak shifted to longer wavelength and the bandgap energy lower. Optical photoluminescence properties confirmed that the UV emission coincides with the green emissions which correspond to the electron transition from the bottom conduction band to Vo, Vzn, and Ozn level. As a result, all the samples of the ZnO NPs have single broad emission in the range of 330nm-550nm with the peak at the UV wavelength of 375nm. Nevertheless, the PL pattern is not linearly with increasing calcination temperature.

Original languageEnglish
Title of host publication8th National Physics Seminar 2019
EditorsFauzi Bakri, Firmanul Catur Wibowo, Iwan Sugihartono, Esmar Budi, Widyaningrum Indrasari, Umiatin, Teguh Budi Prayitno
PublisherAmerican Institute of Physics Inc.
ISBN (Electronic)9780735419162
DOIs
Publication statusPublished - 7 Nov 2019
Event8th National Physics Seminar 2019 - Jakarta, Indonesia
Duration: 29 Jun 201930 Jun 2019

Publication series

NameAIP Conference Proceedings
Volume2169
ISSN (Print)0094-243X
ISSN (Electronic)1551-7616

Conference

Conference8th National Physics Seminar 2019
Country/TerritoryIndonesia
CityJakarta
Period29/06/1930/06/19

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