TY - GEN
T1 - Synthesis of TiO2 from TiOSO4 Solution with Sonochemical Method
AU - Yustanti, Erlina
AU - Syihab, Muhammad Zuhdi
AU - Lalasari, Latifa Hanum
AU - Manaf, Azwar
N1 - Funding Information:
The authors gratefully acknowledge the support of Research Center for Metallurgy and Materials, National Research and Innovation Agency (BRIN) Serpong and Nanomaterial and Process Technology Laboratory, Centre of Excellence, Faculty of Engineering, Sultan Ageng Tirtayasa University for the research facilites. We would also like to thank Physics Department of the Universitas Indonesia for access to the LS100Q Laser Diffraction Particle Size Analyzer, Beckman Coulter facilities.
Publisher Copyright:
© 2022 Trans Tech Publications Ltd, Switzerland.
PY - 2022/3
Y1 - 2022/3
N2 - TiO2 is a semiconductor that possesses superior chemical and physical properties, widely used in various fields. In this research, the synthesis of TiO2 particles was carried out by the sonochemical method. Synthesis begins by mixing the precursor TiOSO4 in H2O with a ratio of the solvent volume (v/v) H2O/TiOSO4 20-80. TiO2 particles through sonochemically reduced for 15-75 minutes. Changes in particle diameter during the synthesis process are calculated by particle size analyzer. The results of the particle size analyzer showed that the increase in the solvent volume ratio causes the average diameter of TiO2 particles to increase with a heterogeneous size distribution. Conversely, the increasing time on sonochemical processing causes a very significant decrease in the average particle diameter. The best parameter in the sonochemical method was the lowest solvent volume ratio, 20, and the sonochemical time process of 75 minutes generated a single anatase phase 338 nm with a spherical shape.
AB - TiO2 is a semiconductor that possesses superior chemical and physical properties, widely used in various fields. In this research, the synthesis of TiO2 particles was carried out by the sonochemical method. Synthesis begins by mixing the precursor TiOSO4 in H2O with a ratio of the solvent volume (v/v) H2O/TiOSO4 20-80. TiO2 particles through sonochemically reduced for 15-75 minutes. Changes in particle diameter during the synthesis process are calculated by particle size analyzer. The results of the particle size analyzer showed that the increase in the solvent volume ratio causes the average diameter of TiO2 particles to increase with a heterogeneous size distribution. Conversely, the increasing time on sonochemical processing causes a very significant decrease in the average particle diameter. The best parameter in the sonochemical method was the lowest solvent volume ratio, 20, and the sonochemical time process of 75 minutes generated a single anatase phase 338 nm with a spherical shape.
KW - sonochemical
KW - TiOSO
KW - titanium dioxide
UR - http://www.scopus.com/inward/record.url?scp=85128803472&partnerID=8YFLogxK
U2 - 10.4028/p-g9k5mq
DO - 10.4028/p-g9k5mq
M3 - Conference contribution
AN - SCOPUS:85128803472
SN - 9783035717723
T3 - Materials Science Forum
SP - 243
EP - 254
BT - Broad Exposure to Science and Technology II - Selected peer-reviewed full text papers from the Broad Exposure to Science and Technology, BEST 2021
A2 - Wardhono, Endarto Y.
PB - Trans Tech Publications Ltd
T2 - Conference on Broad Exposure to Science and Technology, BEST 2021
Y2 - 31 August 2021 through 31 August 2021
ER -