Synthesis of imidazoline-palmitic derivative using MAOS (microwave assisted organic synthesis) method

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Abstract

In this work, imidazoline-palmitic derivative had been successfully synthesized by reacting triethylenetetramine (TETA) with palmitic acid (PA). Synthesis process was performed with solvent free using MAOS (Microwave Assisted Organic Synthesis) method with variation of time reactions. Dean-Stark and reflux methods using xylene as a solvent were also performed as comparisons. The percentage yield of TETA-PA imidazoline was obtained from Dean-Stark at 13 hours (95.80 %), reflux at 13 hours (88.53 %), and MAOS at 11 min (87.74 %). TETA-PA imidazoline then was identified by using thin layer chromatography and melting point analyzer followed by characterization using Fourier Transform Infrared (FTIR), UV-Vis, Proton Nuclear Magnetic Resonance (1H-NMR), and Mass Spectrometry (MS) spectral data. This study provides information regarding comparison method for imidazoline derivative synthesis. For further research, TETA-PA imidazoline can be used as corrosion inhibitor towards carbon steel.

Original languageEnglish
Article number012006
JournalIOP Conference Series: Materials Science and Engineering
Volume763
Issue number1
DOIs
Publication statusPublished - 28 Apr 2020
Event3rd International Symposium on Current Progress in Functional Materials 2018, ISCPFM 2018 - Depok, Indonesia
Duration: 8 Aug 20189 Aug 2018

Keywords

  • corrosion inhibitor
  • imidazoline
  • MAOS
  • palmitic acid
  • triethylenetetramine

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