Synthesis of ACNT on quartz substrate with catalytic decomposition reaction from Cinnamomum camphora by using FC-CVD method

Praswasti Pembangun Dyah Kencana Wulan, Toni Partogi Johannes Silaen

Research output: Chapter in Book/Report/Conference proceedingConference contributionpeer-review

5 Citations (Scopus)

Abstract

Camphor is a renewable carbon source that can be used as raw material for synthesizing Carbon Nanotube (CNT). Camphor is a substance that can be found on the Cinnamomum camphora tree. In this research, the method used to synthesize Aligned Carbon Nanotube (ACNT) from camphor is Floating Catalyst Chemical Vapor Deposition (FC-CVD) with Ferrocene as catalyst at temperature of 800°C, hydrogen gas as the co-reactant and argon gas as carrier gas. This method is the most popular method of synthesizing ACNT which oriented and have a high density. Camphor decomposes into benzene, toluene, and xylene at a temperature of 800°C. By using GC-FID for characterization test, the results showed decomposition at a temperature of 800°C camphor dominated by benzene with a concentration of 92.422 to 97.656%. The research was conducted by varying the flow rate of carrier gas such as argon at 40, 55, 70, 85 and 100 mL / min at a temperature of 800°C for 60 minutes of reaction time. Argon carrier gas flow rate of 70 mL / min producing CNT with the highest yield, but this is not followed by best quality of CNT. CNT with best quality is obtained at a flow rate of argon carrier gas at 55 mL / min based on test results characterization by using SEM, EDX, Mapping, and RAMAN Spectroscopy. This research have not obtained CNT with aligned structured.

Original languageEnglish
Title of host publicationInternational Seminar on Fundamental and Application of Chemical Engineering 2016, ISFAChE 2016
Subtitle of host publicationProceedings of the 3rd International Seminar on Fundamental and Application of Chemical Engineering 2016
Editors Widiyastuti, Fadlilatul Taufany, Siti Nurkhamidah
PublisherAmerican Institute of Physics Inc.
ISBN (Electronic)9780735415102
DOIs
Publication statusPublished - 24 May 2017
Event3rd International Seminar on Fundamental and Application of Chemical Engineering 2016, ISFAChE 2016 - East Java, Indonesia
Duration: 1 Nov 20162 Nov 2016

Publication series

NameAIP Conference Proceedings
Volume1840
ISSN (Print)0094-243X
ISSN (Electronic)1551-7616

Conference

Conference3rd International Seminar on Fundamental and Application of Chemical Engineering 2016, ISFAChE 2016
CountryIndonesia
CityEast Java
Period1/11/162/11/16

Keywords

  • Cinnamomum Camphora
  • CNT
  • FC-CVD
  • Ferrocene
  • Quartz

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