Synthesis and characterization of Ni nanoparticles supported on nitrogen-doped mesoporous carbon

A. Z. Pamungkas, I. Abdullah, Y. K. Krisnandi

Research output: Contribution to journalConference articlepeer-review

5 Citations (Scopus)

Abstract

Nitrogen-doped mesoporous carbon (N-MC) was synthesized by the soft-templating method using phloroglucinol/formaldehyde and melamine as carbon and nitrogen precursors, respectively, and Pluronic F127 as a template for the generation of mesopores inside the carbon structure. Scanning electron microscopy analysis revealed that the material had a rough surface, while Raman analysis indicated the existence of sp2-hybridized carbon rather than sp3, similar to graphite. The increase of the D-band to G-band intensity ratio indicated that N-MC has a more graphite-like structure than pristine mesoporous carbon. X-ray photoelectron spectroscopy analysis confirmed that nitrogen was successfully doped into the carbon framework. The material was then used as a support for Ni nanoparticles (Ni-NPs). The presence of Ni metal in Ni-NP@N-MC was confirmed by X-ray diffraction analysis.

Original languageEnglish
Article number012003
JournalIOP Conference Series: Materials Science and Engineering
Volume496
Issue number1
DOIs
Publication statusPublished - 22 Feb 2019
Event2nd International Conference on Current Progress in Functional Materials 2017, ISCPFM 2017 - Bali, Indonesia
Duration: 8 Nov 20179 Nov 2017

Keywords

  • mesoporous carbon
  • N-doped carbon
  • Ni nanoparticles
  • soft-templating method

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