Preparation of gold-palladium modified boron-doped diamond electrode and its preliminary test for oxygen sensors

M. S.P. Luhur, T. A. Ivandini, M. Khalil

Research output: Chapter in Book/Report/Conference proceedingConference contributionpeer-review

5 Citations (Scopus)

Abstract

Core shell Au@Pd nanoparticles modified at boron-doped diamond (AuPd-BDD) electrodes were successfully prepared. Pd shell was formed at Au nanoparticles (AuNP) by the reduction reaction of H2PdCl4 to produce purple Au@Pd nanoparticles. The characterization performed using UV-Visible spectrophotometer showed the maximum wavelength at 523 nm, which decreased with the formation of Pd shell. The AuPd was then deposited on N-BDD surfaces and characterized using scanning electron microscopy (SEM) and X-Ray photoelectron spectroscopy (XPS). The modified electrode was used to determine the oxygen dissolved in phosphate buffer solution (PBS) by using cyclic voltammetry technique. Comparison between voltammograms of AuPd-N-BDD and AuNP-N-BDD indicated that the deposition of Au@Pd nanoparticles on N-BDD was successfully performed.

Original languageEnglish
Title of host publicationProceedings of the 3rd International Symposium on Current Progress in Mathematics and Sciences 2017, ISCPMS 2017
EditorsRatna Yuniati, Terry Mart, Ivandini T. Anggraningrum, Djoko Triyono, Kiki A. Sugeng
PublisherAmerican Institute of Physics Inc.
ISBN (Electronic)9780735417410
DOIs
Publication statusPublished - 22 Oct 2018
Event3rd International Symposium on Current Progress in Mathematics and Sciences 2017, ISCPMS 2017 - Bali, Indonesia
Duration: 26 Jul 201727 Jul 2017

Publication series

NameAIP Conference Proceedings
Volume2023
ISSN (Print)0094-243X
ISSN (Electronic)1551-7616

Conference

Conference3rd International Symposium on Current Progress in Mathematics and Sciences 2017, ISCPMS 2017
Country/TerritoryIndonesia
CityBali
Period26/07/1727/07/17

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