TY - JOUR
T1 - PREPARATION of [BzMe3N]2[Na2W4O12(OMe)4(MeOH)6].6MeOH
AU - Bakri, Ridla
PY - 2003
Y1 - 2003
N2 - Anattempt to prepare trinuclear tungsten oxoalkoxides [BzMe3N]3[W3O8(OMe)5] from the reaction between WO2(OMe)2, [BzMe3N]2WO4 and [BzMe3N](OMe) in the ratio of 2:1:1 in MeOH produced [BzMe3N]2[Na2W4O12(OMe)4(MeOH)6].6MeOH. Suitable crystals for X-ray chrystallographic studies were obtained from hot mixture of methanol-acetonitrile solution. The I.R., 1H-NMR, and microanalysis data including crystal structure of [Na2W4O12(OMe)4(MeOH)6]2- anion are reported.
AB - Anattempt to prepare trinuclear tungsten oxoalkoxides [BzMe3N]3[W3O8(OMe)5] from the reaction between WO2(OMe)2, [BzMe3N]2WO4 and [BzMe3N](OMe) in the ratio of 2:1:1 in MeOH produced [BzMe3N]2[Na2W4O12(OMe)4(MeOH)6].6MeOH. Suitable crystals for X-ray chrystallographic studies were obtained from hot mixture of methanol-acetonitrile solution. The I.R., 1H-NMR, and microanalysis data including crystal structure of [Na2W4O12(OMe)4(MeOH)6]2- anion are reported.
UR - http://journal.ui.ac.id/index.php/science/article/view/290
U2 - 10.7454/mss.v7i1.290
DO - 10.7454/mss.v7i1.290
M3 - Article
SN - 1693-6671
VL - 7
JO - MAKARA of Science Series
JF - MAKARA of Science Series
IS - 1
ER -