Effect of the quantity of carbonate components and sintering parameters on the quality of hydrothermally synthesized carbonate hydroxyapatite

A. A. Ruddyard, Djarwani Soeharso Soejoko, Nurlely

Research output: Chapter in Book/Report/Conference proceedingConference contributionpeer-review

Abstract

Carbonated hydroxyapatite is a biomaterial with high biocompatibility with human bone, moreso than regular hydroxyapatite, making it an acceptable synthetic bone graft material. The purpose of this research is to study the effect of sintering temperature and time on carbonated hydroxyapatite samples synthesized using a hydrothermal method with CaCO3 as one of its components. The samples are then characterized using Fourier-Transform Infrared Spectroscopy, X-Ray Diffraction, and Scanning Electron Microscope. Infrared (IR) spectra showed that the CO3 content in each sample is proportional to the amount of CaCO3 used during synthesis. X-Ray Diffraction (XRD) patterns showed an increase in apatite content and a decrease in calcite content as sintering temperature and time increases, with temperature increases having a stronger effect on the samples than time increases. Calcite disappears completely after sintering at 900 °C for 2 hours.

Original languageEnglish
Title of host publicationInternational Symposium on Current Progress in Mathematics and Sciences 2016, ISCPMS 2016
Subtitle of host publicationProceedings of the 2nd International Symposium on Current Progress in Mathematics and Sciences 2016
EditorsKiki Ariyanti Sugeng, Djoko Triyono, Terry Mart
PublisherAmerican Institute of Physics Inc.
ISBN (Electronic)9780735415362
DOIs
Publication statusPublished - 10 Jul 2017
Event2nd International Symposium on Current Progress in Mathematics and Sciences 2016, ISCPMS 2016 - Depok, Jawa Barat, Indonesia
Duration: 1 Nov 20162 Nov 2016

Publication series

NameAIP Conference Proceedings
Volume1862
ISSN (Print)0094-243X
ISSN (Electronic)1551-7616

Conference

Conference2nd International Symposium on Current Progress in Mathematics and Sciences 2016, ISCPMS 2016
Country/TerritoryIndonesia
CityDepok, Jawa Barat
Period1/11/162/11/16

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