Crude glycerol from waste cooking oil treatment as an alternative solvent in synthesis of diethyl-2,6-dimethyl-4-phenyl-1,4-dihydropyridine-3,5-dicarboxylate

A. H. Cahyana; B. Ardiansah; H. Hanifah

doi:10.1088/1757-899X/763/1/012016

Crude glycerol from waste cooking oil treatment as an alternative solvent in synthesis of diethyl-2,6-dimethyl-4-phenyl-1,4-dihydropyridine-3,5-dicarboxylate

A. H. Cahyana, B. Ardiansah, H. Hanifah

Department of Chemistry

Research output: Contribution to journal › Conference article › peer-review

Abstract

Diethyl-2,6-dimethyl-4-phenyl-1,4-dihydropyridine-3,5-dicarboxylate, a 1,4-DHP derivative, has been synthesized from benzaldehyde, ethyl acetoacetate and ammonium acetate via a one-pot three component reaction in crude glycerol as solvent. Crude glycerol was obtained from the treatment of waste cooking oil. The product was obtained in 69 % yield when the reaction was conducted at 90 °C for 1 h under reflux in 10 mL glycerol.

Original language	English
Article number	012016
Journal	IOP Conference Series: Materials Science and Engineering
Volume	763
Issue number	1
DOIs	https://doi.org/10.1088/1757-899X/763/1/012016
Publication status	Published - 28 Apr 2020
Event	3rd International Symposium on Current Progress in Functional Materials 2018, ISCPFM 2018 - Depok, Indonesia Duration: 8 Aug 2018 → 9 Aug 2018

Keywords

4-dihydropyridine
glycerol
hydrolysis
solvent
waste cooking oil

Access to Document

10.1088/1757-899X/763/1/012016

Cite this

@article{d6b793dfddc240a481d704f97c24219a,

title = "Crude glycerol from waste cooking oil treatment as an alternative solvent in synthesis of diethyl-2,6-dimethyl-4-phenyl-1,4-dihydropyridine-3,5-dicarboxylate",

abstract = "Diethyl-2,6-dimethyl-4-phenyl-1,4-dihydropyridine-3,5-dicarboxylate, a 1,4-DHP derivative, has been synthesized from benzaldehyde, ethyl acetoacetate and ammonium acetate via a one-pot three component reaction in crude glycerol as solvent. Crude glycerol was obtained from the treatment of waste cooking oil. The product was obtained in 69 % yield when the reaction was conducted at 90 °C for 1 h under reflux in 10 mL glycerol.",

keywords = "4-dihydropyridine, glycerol, hydrolysis, solvent, waste cooking oil",

author = "Cahyana, {A. H.} and B. Ardiansah and H. Hanifah",

note = "Publisher Copyright: {\textcopyright} 2020 Published under licence by IOP Publishing Ltd.; 3rd International Symposium on Current Progress in Functional Materials 2018, ISCPFM 2018 ; Conference date: 08-08-2018 Through 09-08-2018",

year = "2020",

month = apr,

day = "28",

doi = "10.1088/1757-899X/763/1/012016",

language = "English",

volume = "763",

journal = "IOP Conference Series: Materials Science and Engineering",

issn = "1757-8981",

publisher = "IOP Publishing Ltd.",

number = "1",

}

Crude glycerol from waste cooking oil treatment as an alternative solvent in synthesis of diethyl-2,6-dimethyl-4-phenyl-1,4-dihydropyridine-3,5-dicarboxylate. / Cahyana, A. H.; Ardiansah, B.; Hanifah, H.
In: IOP Conference Series: Materials Science and Engineering, Vol. 763, No. 1, 012016, 28.04.2020.

Research output: Contribution to journal › Conference article › peer-review

TY - JOUR

T1 - Crude glycerol from waste cooking oil treatment as an alternative solvent in synthesis of diethyl-2,6-dimethyl-4-phenyl-1,4-dihydropyridine-3,5-dicarboxylate

AU - Cahyana, A. H.

AU - Ardiansah, B.

AU - Hanifah, H.

PY - 2020/4/28

Y1 - 2020/4/28

N2 - Diethyl-2,6-dimethyl-4-phenyl-1,4-dihydropyridine-3,5-dicarboxylate, a 1,4-DHP derivative, has been synthesized from benzaldehyde, ethyl acetoacetate and ammonium acetate via a one-pot three component reaction in crude glycerol as solvent. Crude glycerol was obtained from the treatment of waste cooking oil. The product was obtained in 69 % yield when the reaction was conducted at 90 °C for 1 h under reflux in 10 mL glycerol.

AB - Diethyl-2,6-dimethyl-4-phenyl-1,4-dihydropyridine-3,5-dicarboxylate, a 1,4-DHP derivative, has been synthesized from benzaldehyde, ethyl acetoacetate and ammonium acetate via a one-pot three component reaction in crude glycerol as solvent. Crude glycerol was obtained from the treatment of waste cooking oil. The product was obtained in 69 % yield when the reaction was conducted at 90 °C for 1 h under reflux in 10 mL glycerol.

KW - 4-dihydropyridine

KW - glycerol

KW - hydrolysis

KW - solvent

KW - waste cooking oil

UR - http://www.scopus.com/inward/record.url?scp=85084321095&partnerID=8YFLogxK

U2 - 10.1088/1757-899X/763/1/012016

DO - 10.1088/1757-899X/763/1/012016

M3 - Conference article

AN - SCOPUS:85084321095

SN - 1757-8981

VL - 763

JO - IOP Conference Series: Materials Science and Engineering

JF - IOP Conference Series: Materials Science and Engineering

IS - 1

M1 - 012016

T2 - 3rd International Symposium on Current Progress in Functional Materials 2018, ISCPFM 2018

Y2 - 8 August 2018 through 9 August 2018

ER -

Crude glycerol from waste cooking oil treatment as an alternative solvent in synthesis of diethyl-2,6-dimethyl-4-phenyl-1,4-dihydropyridine-3,5-dicarboxylate

Abstract

Keywords

Access to Document

Other files and links

Fingerprint

Cite this