TY - JOUR
T1 - Crude glycerol from waste cooking oil treatment as an alternative solvent in synthesis of diethyl-2,6-dimethyl-4-phenyl-1,4-dihydropyridine-3,5-dicarboxylate
AU - Cahyana, A. H.
AU - Ardiansah, B.
AU - Hanifah, H.
N1 - Funding Information:
Ac k n o wle d g e m e n ts This work was supported by PITTA Grant 2018 from Universitas Indonesia with contract No. 234/UN2.R3.1/PPM.00/2018.
Publisher Copyright:
© 2020 Published under licence by IOP Publishing Ltd.
PY - 2020/4/28
Y1 - 2020/4/28
N2 - Diethyl-2,6-dimethyl-4-phenyl-1,4-dihydropyridine-3,5-dicarboxylate, a 1,4-DHP derivative, has been synthesized from benzaldehyde, ethyl acetoacetate and ammonium acetate via a one-pot three component reaction in crude glycerol as solvent. Crude glycerol was obtained from the treatment of waste cooking oil. The product was obtained in 69 % yield when the reaction was conducted at 90 °C for 1 h under reflux in 10 mL glycerol.
AB - Diethyl-2,6-dimethyl-4-phenyl-1,4-dihydropyridine-3,5-dicarboxylate, a 1,4-DHP derivative, has been synthesized from benzaldehyde, ethyl acetoacetate and ammonium acetate via a one-pot three component reaction in crude glycerol as solvent. Crude glycerol was obtained from the treatment of waste cooking oil. The product was obtained in 69 % yield when the reaction was conducted at 90 °C for 1 h under reflux in 10 mL glycerol.
KW - 4-dihydropyridine
KW - glycerol
KW - hydrolysis
KW - solvent
KW - waste cooking oil
UR - http://www.scopus.com/inward/record.url?scp=85084321095&partnerID=8YFLogxK
U2 - 10.1088/1757-899X/763/1/012016
DO - 10.1088/1757-899X/763/1/012016
M3 - Conference article
AN - SCOPUS:85084321095
SN - 1757-8981
VL - 763
JO - IOP Conference Series: Materials Science and Engineering
JF - IOP Conference Series: Materials Science and Engineering
IS - 1
M1 - 012016
T2 - 3rd International Symposium on Current Progress in Functional Materials 2018, ISCPFM 2018
Y2 - 8 August 2018 through 9 August 2018
ER -