5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl phenyl acetate

Maya Damayanti Rahayu; Susi Kusumaningrum; Hayun Hayun

doi:10.3390/M1041

5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl phenyl acetate

Maya Damayanti Rahayu
, Susi Kusumaningrum
, Hayun Hayun

Department of Pharmacy

Research output: Contribution to journal › Article › peer-review

1 Citation (Scopus)

Abstract

We synthesized a novel compound, 5-(6-hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methylphenyl acetate, in a good yield by oxidation of 1-O-acetyl-xanthorrizol using potassium permanganate in acidic condition. The structure was elucidated by Fourier Transform Infrared (FTIR), ¹ H-Nuclear Magnetic Resonance (NMR) and ¹³ C-NMR, two-dimensional (2D)-HSQC, Distortionless Enhancement by Polarization Transfer (DEPT), 2D-Heteronuclear Multiple Bond Correlation (HMBC), and High-Resolution Mass Spectra (HRMS) spectral data.

Original language	English
Article number	M1041
Journal	MolBank
Volume	2019
Issue number	1
DOIs	https://doi.org/10.3390/M1041
Publication status	Published - 1 Mar 2019

Keywords

1-O-acetyl-xanthorrhizol
Oxidation
Potassium permanganate
Xanthorrizol

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10.3390/M1041

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title = "5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl phenyl acetate",

abstract = " We synthesized a novel compound, 5-(6-hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methylphenyl acetate, in a good yield by oxidation of 1-O-acetyl-xanthorrizol using potassium permanganate in acidic condition. The structure was elucidated by Fourier Transform Infrared (FTIR), 1 H-Nuclear Magnetic Resonance (NMR) and 13 C-NMR, two-dimensional (2D)-HSQC, Distortionless Enhancement by Polarization Transfer (DEPT), 2D-Heteronuclear Multiple Bond Correlation (HMBC), and High-Resolution Mass Spectra (HRMS) spectral data. ",

keywords = "1-O-acetyl-xanthorrhizol, Oxidation, Potassium permanganate, Xanthorrizol",

author = "Rahayu, \{Maya Damayanti\} and Susi Kusumaningrum and Hayun Hayun",

note = "Publisher Copyright: {\textcopyright} 2018 by the authors. Licensee MDPI, Basel, Switzerland.",

year = "2019",

month = mar,

day = "1",

doi = "10.3390/M1041",

language = "English",

volume = "2019",

journal = "MolBank",

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TY - JOUR

T1 - 5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl phenyl acetate

AU - Rahayu, Maya Damayanti

AU - Kusumaningrum, Susi

AU - Hayun, Hayun

PY - 2019/3/1

Y1 - 2019/3/1

N2 - We synthesized a novel compound, 5-(6-hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methylphenyl acetate, in a good yield by oxidation of 1-O-acetyl-xanthorrizol using potassium permanganate in acidic condition. The structure was elucidated by Fourier Transform Infrared (FTIR), 1 H-Nuclear Magnetic Resonance (NMR) and 13 C-NMR, two-dimensional (2D)-HSQC, Distortionless Enhancement by Polarization Transfer (DEPT), 2D-Heteronuclear Multiple Bond Correlation (HMBC), and High-Resolution Mass Spectra (HRMS) spectral data.

AB - We synthesized a novel compound, 5-(6-hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methylphenyl acetate, in a good yield by oxidation of 1-O-acetyl-xanthorrizol using potassium permanganate in acidic condition. The structure was elucidated by Fourier Transform Infrared (FTIR), 1 H-Nuclear Magnetic Resonance (NMR) and 13 C-NMR, two-dimensional (2D)-HSQC, Distortionless Enhancement by Polarization Transfer (DEPT), 2D-Heteronuclear Multiple Bond Correlation (HMBC), and High-Resolution Mass Spectra (HRMS) spectral data.

KW - 1-O-acetyl-xanthorrhizol

KW - Oxidation

KW - Potassium permanganate

KW - Xanthorrizol

UR - https://www.scopus.com/pages/publications/85063586293

U2 - 10.3390/M1041

DO - 10.3390/M1041

M3 - Article

AN - SCOPUS:85063586293

SN - 1422-8599

VL - 2019

JO - MolBank

JF - MolBank

IS - 1

M1 - M1041

ER -

5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl phenyl acetate

Abstract

Keywords

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