TY - JOUR
T1 - 5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl phenyl acetate
AU - Rahayu, Maya Damayanti
AU - Kusumaningrum, Susi
AU - Hayun, Hayun
N1 - Funding Information:
Acknowledgments: The authors are grateful to the Directorate of Research and Community Services, Universitas Indonesia, Depok, Indonesia, for the financial support of this study. Additional thanks go out to the Synthesis Laboratory, Center of Pharmaceutical and Medical Technology, The Agency for the Assessment and Application of Technology (BPPT), Republic of Indonesia, for providing the facilities for this study; to the Chemistry Study Program, Faculty of Natural Sciences, Bandung Institute of Technology (ITB), Bandung, Indonesia, for recording NMR and HR-MS spectra; and to the Ministry of Research, Technology, and Higher Education of the Republic of Indonesia, for the provision of Science and Technology Scholarship (to M.D. Rahayu).
Funding Information:
This research was funded by Programme of International Indexed Publication Grants for Student Final Assignments (PITTA Grant) Fiscal Year 2018, Universitas Indonesia, grant number 1768/UN2.R3.1/HKP.05.00/2018. The APC was funded by Universitas Indonesia.
Publisher Copyright:
© 2018 by the authors. Licensee MDPI, Basel, Switzerland.
PY - 2019/3/1
Y1 - 2019/3/1
N2 -
We synthesized a novel compound, 5-(6-hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methylphenyl acetate, in a good yield by oxidation of 1-O-acetyl-xanthorrizol using potassium permanganate in acidic condition. The structure was elucidated by Fourier Transform Infrared (FTIR),
1
H-Nuclear Magnetic Resonance (NMR) and
13
C-NMR, two-dimensional (2D)-HSQC, Distortionless Enhancement by Polarization Transfer (DEPT), 2D-Heteronuclear Multiple Bond Correlation (HMBC), and High-Resolution Mass Spectra (HRMS) spectral data.
AB -
We synthesized a novel compound, 5-(6-hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methylphenyl acetate, in a good yield by oxidation of 1-O-acetyl-xanthorrizol using potassium permanganate in acidic condition. The structure was elucidated by Fourier Transform Infrared (FTIR),
1
H-Nuclear Magnetic Resonance (NMR) and
13
C-NMR, two-dimensional (2D)-HSQC, Distortionless Enhancement by Polarization Transfer (DEPT), 2D-Heteronuclear Multiple Bond Correlation (HMBC), and High-Resolution Mass Spectra (HRMS) spectral data.
KW - 1-O-acetyl-xanthorrhizol
KW - Oxidation
KW - Potassium permanganate
KW - Xanthorrizol
UR - http://www.scopus.com/inward/record.url?scp=85063586293&partnerID=8YFLogxK
U2 - 10.3390/M1041
DO - 10.3390/M1041
M3 - Article
AN - SCOPUS:85063586293
SN - 1422-8599
VL - 2019
JO - MolBank
JF - MolBank
IS - 1
M1 - M1041
ER -