5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl phenyl acetate

Maya Damayanti Rahayu, Susi Kusumaningrum, Hayun Hayun

Research output: Contribution to journalArticleResearchpeer-review

Abstract

We synthesized a novel compound, 5-(6-hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methylphenyl acetate, in a good yield by oxidation of 1-O-acetyl-xanthorrizol using potassium permanganate in acidic condition. The structure was elucidated by Fourier Transform Infrared (FTIR), 1 H-Nuclear Magnetic Resonance (NMR) and 13 C-NMR, two-dimensional (2D)-HSQC, Distortionless Enhancement by Polarization Transfer (DEPT), 2D-Heteronuclear Multiple Bond Correlation (HMBC), and High-Resolution Mass Spectra (HRMS) spectral data.

Original languageEnglish
Article numberM1041
JournalMolBank
Volume2019
Issue number1
DOIs
Publication statusPublished - 1 Mar 2019

Fingerprint

acetates
Magnetic Resonance Spectroscopy
Nuclear magnetic resonance
Potassium Permanganate
nuclear magnetic resonance
Fourier Analysis
mass spectra
potassium
Fourier transforms
Acetates
Polarization
Infrared radiation
Oxidation
oxidation
augmentation
high resolution
polarization
phenyl acetate
methyl acetate
xanthorrhizol

Keywords

  • 1-O-acetyl-xanthorrhizol
  • Oxidation
  • Potassium permanganate
  • Xanthorrizol

Cite this

Rahayu, Maya Damayanti ; Kusumaningrum, Susi ; Hayun, Hayun. / 5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl phenyl acetate. In: MolBank. 2019 ; Vol. 2019, No. 1.
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abstract = "We synthesized a novel compound, 5-(6-hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methylphenyl acetate, in a good yield by oxidation of 1-O-acetyl-xanthorrizol using potassium permanganate in acidic condition. The structure was elucidated by Fourier Transform Infrared (FTIR), 1 H-Nuclear Magnetic Resonance (NMR) and 13 C-NMR, two-dimensional (2D)-HSQC, Distortionless Enhancement by Polarization Transfer (DEPT), 2D-Heteronuclear Multiple Bond Correlation (HMBC), and High-Resolution Mass Spectra (HRMS) spectral data.",
keywords = "1-O-acetyl-xanthorrhizol, Oxidation, Potassium permanganate, Xanthorrizol",
author = "Rahayu, {Maya Damayanti} and Susi Kusumaningrum and Hayun Hayun",
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5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl phenyl acetate. / Rahayu, Maya Damayanti; Kusumaningrum, Susi; Hayun, Hayun.

In: MolBank, Vol. 2019, No. 1, M1041, 01.03.2019.

Research output: Contribution to journalArticleResearchpeer-review

TY - JOUR

T1 - 5-(6-Hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methyl phenyl acetate

AU - Rahayu, Maya Damayanti

AU - Kusumaningrum, Susi

AU - Hayun, Hayun

PY - 2019/3/1

Y1 - 2019/3/1

N2 - We synthesized a novel compound, 5-(6-hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methylphenyl acetate, in a good yield by oxidation of 1-O-acetyl-xanthorrizol using potassium permanganate in acidic condition. The structure was elucidated by Fourier Transform Infrared (FTIR), 1 H-Nuclear Magnetic Resonance (NMR) and 13 C-NMR, two-dimensional (2D)-HSQC, Distortionless Enhancement by Polarization Transfer (DEPT), 2D-Heteronuclear Multiple Bond Correlation (HMBC), and High-Resolution Mass Spectra (HRMS) spectral data.

AB - We synthesized a novel compound, 5-(6-hydroxy-6-methyl-5-oxoheptan-2-yl)-2-methylphenyl acetate, in a good yield by oxidation of 1-O-acetyl-xanthorrizol using potassium permanganate in acidic condition. The structure was elucidated by Fourier Transform Infrared (FTIR), 1 H-Nuclear Magnetic Resonance (NMR) and 13 C-NMR, two-dimensional (2D)-HSQC, Distortionless Enhancement by Polarization Transfer (DEPT), 2D-Heteronuclear Multiple Bond Correlation (HMBC), and High-Resolution Mass Spectra (HRMS) spectral data.

KW - 1-O-acetyl-xanthorrhizol

KW - Oxidation

KW - Potassium permanganate

KW - Xanthorrizol

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